Information card for entry 4508200

Structure parameters

• Formula: C28 H175 Cu7 Ge4 N28 Na3 O192 W46 Y4
• Calculated formula: C28 H112 Cu7 Ge4 N28 Na3 O180 W46 Y4
• Title of publication: Tetrahedral Polyoxometalate Nanoclusters with Tetrameric Rare-Earth Cores and Germanotungstate Vertexes
• Authors of publication: Zhao, Junwei; Shi, Dongying; Chen, Lijuan; Ma, Pengtao; Wang, Jingping; Zhang, Jian; Niu, Jingyang
• Journal of publication: Crystal Growth & Design
• Year of publication: 2013
• Journal volume: 13
• Journal issue: 10
• Pages of publication: 4368
• a: 21.675 ± 0.002 Å
• b: 23.348 ± 0.002 Å
• c: 24.687 ± 0.002 Å
• α: 93.355 ± 0.002°
• β: 100.387 ± 0.002°
• γ: 97.351 ± 0.002°
• Cell volume: 12144.9 ± 1.8 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1602
• Residual factor for significantly intense reflections: 0.0788
• Weighted residual factors for significantly intense reflections: 0.1306
• Weighted residual factors for all reflections included in the refinement: 0.1397
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No