Syntheses, Structural Variation, and Characterization of a Series of Crystalline Coordination Compounds with 4-Benzene-1,2,4-triazole: Polymorph, Incomplete Spin Transition, and Single Crystal-to-Single Crystal Transformation
Authors of publication
Wu, Xiang Xia; Wang, You You; Yang, Pan; Xu, Yao Yao; Huo, Jian Zhong; Ding, Bin; Wang, Ying; Wang, XiuGuang
Journal of publication
Crystal Growth & Design
Year of publication
2014
Journal volume
14
Journal issue
2
Pages of publication
477
a
16.2395 ± 0.001 Å
b
15.7632 ± 0.001 Å
c
13.9861 ± 0.0009 Å
α
90°
β
102.156 ± 0.001°
γ
90°
Cell volume
3500 ± 0.4 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0764
Residual factor for significantly intense reflections
0.0408
Weighted residual factors for significantly intense reflections
0.0912
Weighted residual factors for all reflections included in the refinement
0.109
Goodness-of-fit parameter for all reflections included in the refinement
