Role of Weak Intermolecular Interactions in the Crystal Structure of Tetrakis-furazano[3,4-c:3′,4′-g:3″,4″-k:3‴,4‴-o][1,2,5,6,9,10,13,14]octaazacyclohexadecine and Its Solvates
Authors of publication
Suponitsky, Kyrill Yu.; Lyssenko, Konstantin A.; Ananyev, Ivan V.; Kozeev, Andrei M.; Sheremetev, Aleksei B.
Journal of publication
Crystal Growth & Design
Year of publication
2014
Journal volume
14
Journal issue
9
Pages of publication
4439
a
15.1136 ± 0.0017 Å
b
6.5756 ± 0.0008 Å
c
18.463 ± 0.002 Å
α
90°
β
113.538 ± 0.002°
γ
90°
Cell volume
1682.2 ± 0.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0633
Residual factor for significantly intense reflections
0.0391
Weighted residual factors for significantly intense reflections
0.0851
Weighted residual factors for all reflections included in the refinement
0.0961
Goodness-of-fit parameter for all reflections included in the refinement
