Information card for entry 4513652

Structure parameters

• Chemical name: cis-dibromido(methyl-4,6-O-benzylidene-2,3-diamino-2,3-dideoxy-alpha-D-glucopyranoside)palladium(II)
• Formula: C14.75 H21.5 Br2 Cl1.5 N2 O4 Pd
• Calculated formula: C14.75 H21.5 Br2 Cl1.5 N2 O4 Pd
• Title of publication: One-Step Preparation and Crystallization of Almost Insoluble Palladium(II) and Platinum(II/IV) Complexes from a Biphasic Solvent System
• Authors of publication: Böge, Matthias; Heck, Jürgen
• Journal of publication: Crystal Growth & Design
• Year of publication: 2015
• Journal volume: 15
• Journal issue: 11
• Pages of publication: 5280
• a: 15.7679 ± 0.0001 Å
• b: 15.7679 ± 0.0001 Å
• c: 32.7215 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8135.44 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 96
• Hermann-Mauguin space group symbol: P 43 21 2
• Hall space group symbol: P 4nw 2abw
• Residual factor for all reflections: 0.0362
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0642
• Weighted residual factors for all reflections included in the refinement: 0.0666
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No