Crystallography Open Database

Information card for entry 4515045

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Coordinates	4515045.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C144 H120 Au8 Cl3 Cu2 P8 Pd
Calculated formula	C144 H120 Au8.316 Cl3 Cu1.684 P8 Pd
Title of publication	Synthesis of Trimetallic (HPd@M<sub>2</sub>Au<sub>8</sub>)<sup>3+</sup> Superatoms (M = Ag, Cu) via Hydride-Mediated Regioselective Doping to (Pd@Au<sub>8</sub>)<sup>2</sup>.
Authors of publication	Hirai, Haru; Takano, Shinjiro; Tsukuda, Tatsuya
Journal of publication	ACS omega
Year of publication	2019
Journal volume	4
Journal issue	4
Pages of publication	7070 - 7075
a	22.193 ± 0.004 Å
b	18.278 ± 0.003 Å
c	34.743 ± 0.006 Å
α	90°
β	96.765 ± 0.003°
γ	90°
Cell volume	13995 ± 4 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1177
Residual factor for significantly intense reflections	0.1013
Weighted residual factors for significantly intense reflections	0.1717
Weighted residual factors for all reflections included in the refinement	0.1788
Goodness-of-fit parameter for all reflections included in the refinement	1.244
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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