Information card for entry 4517839
| Formula |
C23 H28 O2 |
| Calculated formula |
C23 H28 O2 |
| Title of publication |
Palladium-Catalyzed Highly Regioselective Hydrocarboxylation of Alkynes with Carbon Dioxide |
| Authors of publication |
Xiong, Wenfang; Shi, Fuxing; Cheng, Ruixiang; Zhu, Baiyao; Wang, Lu; Chen, Pengquan; Lou, Hongming; Wu, Wanqing; Qi, Chaorong; Lei, Ming; Jiang, Huanfeng |
| Journal of publication |
ACS Catalysis |
| Year of publication |
2020 |
| Pages of publication |
7968 |
| a |
10.0446 ± 0.0007 Å |
| b |
12.2899 ± 0.0007 Å |
| c |
17.0614 ± 0.0009 Å |
| α |
76.398 ± 0.005° |
| β |
74.831 ± 0.005° |
| γ |
88.404 ± 0.005° |
| Cell volume |
1974.5 ± 0.2 Å3 |
| Cell temperature |
100 ± 0.1 K |
| Ambient diffraction temperature |
100 ± 0.1 K |
| Number of distinct elements |
3 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0687 |
| Residual factor for significantly intense reflections |
0.0528 |
| Weighted residual factors for significantly intense reflections |
0.1257 |
| Weighted residual factors for all reflections included in the refinement |
0.1392 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.042 |
| Diffraction radiation probe |
x-ray |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/4517839.html
