Information card for entry 4519257

Structure parameters

• Formula: C20 H30 Ir2 Na3.5 O89 Sb2 W20
• Calculated formula: C20 H30 Ir2 Na3.5 O89 Sb2 W20
• Title of publication: Organorhodium(III)- and Iridium(III)-Substituted 20-Tungstobismuthates(III) and -Antimonates(III), [(MCp*)₂X₂W₂₀O₇₀]^10- (M = Rh^III and Ir^III; X = Bi^III and Sb^III).
• Authors of publication: Mougharbel, Ali S.; Ahmedi, Sihana; Bhattacharya, Saurav; Rajan, Ananthu; Kortz, Ulrich
• Journal of publication: ACS omega
• Year of publication: 2021
• Journal volume: 6
• Journal issue: 50
• Pages of publication: 34494 - 34500
• a: 17.1405 ± 0.0019 Å
• b: 19.507 ± 0.002 Å
• c: 23.73 ± 0.003 Å
• α: 103.028 ± 0.003°
• β: 100.372 ± 0.003°
• γ: 113.516 ± 0.003°
• Cell volume: 6756.7 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1295
• Residual factor for significantly intense reflections: 0.0752
• Weighted residual factors for significantly intense reflections: 0.2071
• Weighted residual factors for all reflections included in the refinement: 0.266
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No