Information card for entry 4519412

Structure parameters

• Formula: C24 H40 Cl6 N4 O8 Si2
• Calculated formula: C23.999 H39.999 Cl5.997 N4 O8 Si2
• Title of publication: Disilanes with Pentacoordinate Si Atoms by Carbon Dioxide Insertion into Aminodisilanes: Syntheses, Molecular Structures, and Dynamic Behavior.
• Authors of publication: Ryll, Christopher; Kraushaar, Konstantin; Wagler, Jörg; Brendler, Erica; Kroke, Edwin
• Journal of publication: ACS omega
• Year of publication: 2022
• Journal volume: 7
• Journal issue: 11
• Pages of publication: 9527 - 9536
• a: 9.773 ± 0.0003 Å
• b: 11.6396 ± 0.0003 Å
• c: 16.0521 ± 0.0005 Å
• α: 86.509 ± 0.002°
• β: 75.909 ± 0.002°
• γ: 86.201 ± 0.002°
• Cell volume: 1765.26 ± 0.09 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0449
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.0909
• Weighted residual factors for all reflections included in the refinement: 0.0949
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No