Syntheses of nido-9,11-X~2~-7,8-C~2~B~9~H~10~- anions (X=Cl, Br or I) and the synthesis and structural characterization of N(C~2~H~5~)~4~[commo-3,3'-Co(4,7-Br~2~-3,1,2-CoC~2~B~9~H~9~)~2~]
Authors of publication
Santos, Erich C.; Pinkerton, Anthony B.; Kinkead, Scott A.; Hurlburt, Paul K.; Jasper, Steve A.; Sellers, Christopher W.; Huffman, John C.; Todd, Lee J.
Journal of publication
Polyhedron
Year of publication
2000
Journal volume
19
Journal issue
15
Pages of publication
1777 - 1781
a
10.66 ± 0.008 Å
b
16.048 ± 0.015 Å
c
8.225 ± 0.005 Å
α
91.49 ± 0.05°
β
105.33 ± 0.04°
γ
72.87 ± 0.05°
Cell volume
1294.8 ± 1.8 Å3
Cell temperature
103.15 K
Ambient diffraction temperature
103.15 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for significantly intense reflections
1.6022
Weighted residual factors for all reflections included in the refinement
0.0482
Goodness-of-fit parameter for all reflections included in the refinement
