Information card for entry 5000401

Structure parameters

• Formula: C27 H60 O P2 Ru Si2
• Calculated formula: C27 H60 O P2 Ru Si2
• Title of publication: Oxidative Addition of a Si‒C(sp) Bond to Ruthenium: Synthesis and Reactivity of Ru(SiMe~3~)(C⋮ CSiMe~3~)(CO)(P^t^Bu~2~Me)~2~}
• Authors of publication: Huang, Dejian; Heyn, Richard H.; Bollinger, John C.; Caulton, Kenneth G.
• Journal of publication: Organometallics
• Year of publication: 1997
• Journal volume: 16
• Journal issue: 3
• Pages of publication: 292 - 293
• a: 11.168 ± 0.002 Å
• b: 18.043 ± 0.004 Å
• c: 17.746 ± 0.004 Å
• α: 90°
• β: 108.03 ± 0.03°
• γ: 90°
• Cell volume: 3400.5 ± 1.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1004
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for all reflections: 0.0916
• Weighted residual factors for significantly intense reflections: 0.0737
• Goodness-of-fit parameter for all reflections: 0.956
• Goodness-of-fit parameter for significantly intense reflections: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No