Information card for entry 7000095

Structure parameters

• Formula: C26 H54 N6 P2 Si2
• Calculated formula: C26 H54 N6 P2 Si2
• SMILES: P1(N(C(C)(C)C)[Si](N1C(C)(C)C)(C)C)Nc1ccccc1NP1N(C(C)(C)C)[Si](N1C(C)(C)C)(C)C
• Title of publication: Reversal of polarization in amidophosphines: neutral- and anionic-kappaP coordination vs. anionic-kappaP,N coordination and the formation of nickelaazaphosphiranes.
• Authors of publication: Schranz, Ingo; Lief, Graham R.; Carrow, Christopher J.; Haagenson, Dana C.; Grocholl, Luke; Stahl, Lothar; Staples, Richard J.; Boomishankar, Ramamoorthy; Steiner, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 20
• Pages of publication: 3307 - 3318
• a: 9.2122 ± 0.0013 Å
• b: 33.045 ± 0.005 Å
• c: 12.3486 ± 0.0016 Å
• α: 90°
• β: 109.808 ± 0.01°
• γ: 90°
• Cell volume: 3536.7 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0693
• Residual factor for significantly intense reflections: 0.0588
• Weighted residual factors for significantly intense reflections: 0.1668
• Weighted residual factors for all reflections included in the refinement: 0.1772
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No