Information card for entry 7000151

Structure parameters

• Formula: C89 H123 F10 N2 Ni2 P4
• Calculated formula: C89 H123 F10 N2 Ni2 P4
• Title of publication: C-F Bond activation at Ni(0) and simple reactions of square planar Ni(II) fluoride complexes.
• Authors of publication: Burling, Suzanne; Elliott, Paul I. P.; Jasim, Naser A.; Lindup, Richard J.; McKenna, Jennifer; Perutz, Robin N.; Archibald, Stephen J.; Whitwood, Adrian C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2005
• Journal issue: 22
• Pages of publication: 3686 - 3695
• a: 14.2302 ± 0.0006 Å
• b: 14.8904 ± 0.0006 Å
• c: 21.0407 ± 0.0009 Å
• α: 87.968 ± 0.001°
• β: 77.025 ± 0.001°
• γ: 76.75 ± 0.001°
• Cell volume: 4228.3 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0656
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.1025
• Weighted residual factors for all reflections included in the refinement: 0.1151
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No