Information card for entry 7000840

Structure parameters

• Common name: [Yb(thf)(Ph3C)(C6H3iPr2NCMeCHCMeNC6H3iPr2)]
• Formula: C52 H64 N2 O Yb
• Calculated formula: C52 H64 N2 O Yb
• Title of publication: Heteroleptic ytterbium(ii) complexes supported by a bulky β-diketiminato ligand
• Authors of publication: Hitchcock, Peter B.; Khvostov, Alexei V.; Lappert, Michael F.; Protchenko, Andrey V.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 13
• Pages of publication: 2383 - 2391
• a: 23.6608 ± 0.0005 Å
• b: 9.0274 ± 0.0002 Å
• c: 21.7827 ± 0.0004 Å
• α: 90°
• β: 100.391 ± 0.001°
• γ: 90°
• Cell volume: 4576.38 ± 0.16 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1021
• Residual factor for significantly intense reflections: 0.0748
• Weighted residual factors for significantly intense reflections: 0.1342
• Weighted residual factors for all reflections included in the refinement: 0.1458
• Goodness-of-fit parameter for all reflections included in the refinement: 1.231
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No