Investigation on the reactivity of dithiophosphonato/dithiophosphato NiII complexes towards 2,4,6-tris-2-pyridyl-1,3,5-triazine: developments and new perspectives
Authors of publication
Aragoni, M. Carla; Arca, Massimiliano; Crespo, Miriam; Devillanova, Francesco A.; Hursthouse, Michael B.; Huth, Susanne L.; Isaia, Francesco; Lippolis, Vito; Verani, Gaetano
Journal of publication
Dalton Transactions
Year of publication
2009
Journal issue
14
Pages of publication
2510 - 2520
a
8.5672 ± 0.0011 Å
b
11.0578 ± 0.0015 Å
c
11.8063 ± 0.0014 Å
α
71.926 ± 0.006°
β
77.024 ± 0.007°
γ
77.929 ± 0.007°
Cell volume
1024.3 ± 0.2 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
6
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.147
Residual factor for significantly intense reflections
0.0867
Weighted residual factors for significantly intense reflections
0.1261
Weighted residual factors for all reflections included in the refinement
0.1456
Goodness-of-fit parameter for all reflections included in the refinement
