Information card for entry 7001309

Structure parameters

• Formula: C92 H82 Ag B5 F20 N28 Ni2 O
• Calculated formula: C92 H80 Ag B5 F20 N28 Ni2 O
• Title of publication: Homonuclear and heteronuclear complexes of a four-armed octadentate ligand: synthetic control based on matching ligand denticity with metal ion coordination preferences
• Authors of publication: Fenton, Hazel; Tidmarsh, Ian S.; Ward, Michael D.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 21
• Pages of publication: 4199 - 4207
• a: 11.5875 ± 0.0004 Å
• b: 18.7782 ± 0.0007 Å
• c: 23.226 ± 0.0008 Å
• α: 77.51 ± 0.002°
• β: 83.373 ± 0.003°
• γ: 86.226 ± 0.003°
• Cell volume: 4896.9 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2078
• Residual factor for significantly intense reflections: 0.09
• Weighted residual factors for significantly intense reflections: 0.2206
• Weighted residual factors for all reflections included in the refinement: 0.2935
• Goodness-of-fit parameter for all reflections included in the refinement: 0.975
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No