Information card for entry 7001348

Structure parameters

• Formula: C22 H24 Cl N3 O P Rh
• Calculated formula: C22 H24 Cl N3 O P Rh
• SMILES: [Rh]1(Cl)([P](c2c([NH]1C)cccc2)(c1c(NC)cccc1)c1c(NC)cccc1)C#[O]
• Title of publication: Mono- and binuclear complexes of rhodium involving a new series of hemilabile o-phosphinoaniline ligands
• Authors of publication: Hounjet, Lindsay J.; Bierenstiel, Matthias; Ferguson, Michael J.; McDonald, Robert; Cowie, Martin
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 21
• Pages of publication: 4213 - 4226
• a: 9.3726 ± 0.0008 Å
• b: 11.3968 ± 0.001 Å
• c: 11.4388 ± 0.001 Å
• α: 85.0063 ± 0.0012°
• β: 77.9072 ± 0.0012°
• γ: 72.8739 ± 0.0011°
• Cell volume: 1141.36 ± 0.17 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0216
• Residual factor for significantly intense reflections: 0.0206
• Weighted residual factors for significantly intense reflections: 0.0569
• Weighted residual factors for all reflections included in the refinement: 0.0576
• Goodness-of-fit parameter for all reflections included in the refinement: 1.104
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No