Information card for entry 7001434

Structure parameters

• Formula: C42 H65 N8 O2.5 Sn2
• Calculated formula: C42 H65 N8 O2.5 Sn2
• Title of publication: Synthesis and characterisation of twelve SnIV diaryls and formation of a SnIII triaryl
• Authors of publication: Hitchcock, Peter B.; Lappert, Michael F.; Pierssens, Luc J.-M.; Protchenko, Andrey V.; Uiterweerd, Patrick G. H.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 23
• Pages of publication: 4578 - 4585
• a: 21.315 ± 0.004 Å
• b: 19.714 ± 0.003 Å
• c: 21.97 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9232 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0612
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.1177
• Weighted residual factors for all reflections included in the refinement: 0.1277
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No