Information card for entry 7001449

Structure parameters

• Formula: C27.5 H23 Cl2 F10 Ge N3
• Calculated formula: C27.5 H23 Cl2 F10 Ge N3
• Title of publication: Novel derivatives of hypervalent germanium: synthesis, structure, and stability
• Authors of publication: Lermontova, El'mira Kh.; Huan, MengMeng; Churakov, Andrei V.; Howard, Judith A. K.; Zabalov, Maxim V.; Karlov, Sergey S.; Zaitseva, Galina S.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 24
• Pages of publication: 4695 - 4702
• a: 7.4562 ± 0.0006 Å
• b: 22.0794 ± 0.0017 Å
• c: 17.7878 ± 0.0014 Å
• α: 90°
• β: 90.241 ± 0.002°
• γ: 90°
• Cell volume: 2928.4 ± 0.4 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0438
• Residual factor for significantly intense reflections: 0.0338
• Weighted residual factors for significantly intense reflections: 0.0817
• Weighted residual factors for all reflections included in the refinement: 0.0846
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No