Information card for entry 7001602

Structure parameters

• Formula: C13 H16 Cl N3 Pd
• Calculated formula: C13 H16 Cl N3 Pd
• Title of publication: A dipalladium complex with a single hydroxo bridge and its methylpalladium precursor
• Authors of publication: Cao, Lingyun; Jennings, Michael C.; Puddephatt, Richard J.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 26
• Pages of publication: 5171 - 5176
• a: 14.7181 ± 0.001 Å
• b: 7.8403 ± 0.0006 Å
• c: 12.0571 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1391.32 ± 0.17 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 20
• Hermann-Mauguin space group symbol: C 2 2 21
• Hall space group symbol: C 2c 2
• Residual factor for all reflections: 0.0269
• Residual factor for significantly intense reflections: 0.0261
• Weighted residual factors for significantly intense reflections: 0.0633
• Weighted residual factors for all reflections included in the refinement: 0.0637
• Goodness-of-fit parameter for all reflections included in the refinement: 1.16
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No