Information card for entry 7001719

Structure parameters

• Formula: Ge2 H24 K14 O86 Pu3 W18
• Calculated formula: Ge2 K14 O86 Pu3 W18
• Title of publication: Probing the 5f electrons in a plutonyl(vi) cluster complex
• Authors of publication: Copping, Roy; Talbot-Eeckelaers, Catherine; Collison, David; Helliwell, Madeleine; Gaunt, Andrew J.; May, Iain; Reilly, Sean D.; Scott, Brian L.; McDonald, Ross D.; Valenzula, Oscar A.; Jones, Chris J.; Sarsfield, Mark J.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 29
• Pages of publication: 5609
• a: 12.11 ± 0.006 Å
• b: 17.799 ± 0.009 Å
• c: 21.571 ± 0.011 Å
• α: 75.251 ± 0.007°
• β: 82.468 ± 0.007°
• γ: 70.2 ± 0.007°
• Cell volume: 4225 ± 4 ų
• Cell temperature: 141 ± 2 K
• Ambient diffraction temperature: 141 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1696
• Residual factor for significantly intense reflections: 0.1175
• Weighted residual factors for significantly intense reflections: 0.1752
• Weighted residual factors for all reflections included in the refinement: 0.1848
• Goodness-of-fit parameter for all reflections included in the refinement: 1.66
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No