Information card for entry 7001723

Structure parameters

• Formula: C10 H14 Cl4 N4 Si2
• Calculated formula: C10 H14 Cl4 N4 Si2
• Title of publication: Syntheses, structures, and reactivity of poly(pyrazolyl)silanes, -disilanes, and the ambidentate κ1Si/κ3N-coordinating tris(3,5-dimethylpyrazolyl)silanide ligand [Si(3,5-Me2pz)3]− (MeTpsd)
• Authors of publication: Armbruster, Felix; Fernández, Ignacio; Breher, Frank
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 29
• Pages of publication: 5612 - 5626
• a: 13.339 ± 0.003 Å
• b: 7.4284 ± 0.0015 Å
• c: 8.6263 ± 0.0017 Å
• α: 90°
• β: 108.76 ± 0.03°
• γ: 90°
• Cell volume: 809.3 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0353
• Residual factor for significantly intense reflections: 0.0302
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0786
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No