Information card for entry 7001725

Structure parameters

• Formula: C19 H29 Li N6 O Si
• Calculated formula: C19 H29 Li N6 O Si
• SMILES: [Si]12=n3n(c(cc3C)C)[Li]([O]3CCCC3)([n]3n2c(cc3C)C)[n]2n1c(cc2C)C
• Title of publication: Syntheses, structures, and reactivity of poly(pyrazolyl)silanes, -disilanes, and the ambidentate κ1Si/κ3N-coordinating tris(3,5-dimethylpyrazolyl)silanide ligand [Si(3,5-Me2pz)3]− (MeTpsd)
• Authors of publication: Armbruster, Felix; Fernández, Ignacio; Breher, Frank
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 29
• Pages of publication: 5612 - 5626
• a: 7.908 ± 0.002 Å
• b: 14.52 ± 0.003 Å
• c: 18.629 ± 0.004 Å
• α: 90°
• β: 95.99 ± 0.03°
• γ: 90°
• Cell volume: 2127.4 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1748
• Residual factor for significantly intense reflections: 0.1338
• Weighted residual factors for significantly intense reflections: 0.2015
• Weighted residual factors for all reflections included in the refinement: 0.2197
• Goodness-of-fit parameter for all reflections included in the refinement: 1.306
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No