Information card for entry 7001854

Structure parameters

• Formula: C16 H100 Co4 N4 Na4 O103 P8 W12
• Calculated formula: C16 H32 Co3.8 N4 Na4 O103.02 P8 W12
• Title of publication: A functional hybrid polyoxometalate framework based on a ‘trilacunary’ heteropolyanion [(P4W6O34)2Co2Na2(H2O)2]18−
• Authors of publication: Ritchie, Chris; Li, Fengyan; Pradeep, Chullikkattil P.; Long, De-Liang; Xu, Lin; Cronin, Leroy
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 33
• Pages of publication: 6483 - 6486
• a: 13.0887 ± 0.0011 Å
• b: 14.9813 ± 0.0014 Å
• c: 17.1216 ± 0.0016 Å
• α: 69.184 ± 0.005°
• β: 70.767 ± 0.005°
• γ: 86.494 ± 0.005°
• Cell volume: 2957.1 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0857
• Residual factor for significantly intense reflections: 0.0626
• Weighted residual factors for significantly intense reflections: 0.1674
• Weighted residual factors for all reflections included in the refinement: 0.1901
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No