Information card for entry 7001860

Structure parameters

• Common name: (Co2IICo2III(HL)2(CH3O)2(N3)3) (1)
• Formula: C29 H52 Cl Co4 N13 O18
• Calculated formula: C28 H38 Cl Co4 N13 O12
• Title of publication: Self-assembly of mixed-valence Co(ii/iii) and Ni(ii) clusters: azide-bridged 1D single chain coordination polymers comprised of tetranuclear units, tetranuclear Co(ii/iii) complexes, ferromagnetically coupled azide-bridged tetranuclear, and hexanuclear Ni(ii) complexes: synthesis, structural, and magnetic properties
• Authors of publication: Tandon, Santokh S.; Bunge, Scott D.; Rakosi, Robert; Xu, Zhiqiang; Thompson, Laurence K.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 33
• Pages of publication: 6536 - 6551
• a: 9.6432 ± 0.0019 Å
• b: 10.269 ± 0.002 Å
• c: 11.465 ± 0.002 Å
• α: 105.953 ± 0.003°
• β: 95.676 ± 0.003°
• γ: 100.701 ± 0.003°
• Cell volume: 1059 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0375
• Residual factor for significantly intense reflections: 0.0288
• Weighted residual factors for significantly intense reflections: 0.0742
• Weighted residual factors for all reflections included in the refinement: 0.083
• Goodness-of-fit parameter for all reflections included in the refinement: 0.477
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No