Information card for entry 7002305

Structure parameters

• Formula: C49 H65 N4 P2 Si3 Sn
• Calculated formula: C49 H65 N4 P2 Si3 Sn
• Title of publication: Synthesis and characterization of Sn(II), Pb(II) and Yb(II) complexes supported by [C(Ph2PNSiMe3){6-(2-RC5H3N)}]2− or [CH(Ph2PNSiMe3){6-(2-RC5H3N)}]− (R = 3,5-dimethyl-1-pyrazolyl or iminophosphoranyl) ligands
• Authors of publication: Chai, Zuo-Yun; Wang, Zhong-Xia
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 38
• Pages of publication: 8005 - 8012
• a: 10.4319 ± 0.0016 Å
• b: 15.457 ± 0.003 Å
• c: 17.668 ± 0.003 Å
• α: 80.404 ± 0.003°
• β: 72.936 ± 0.003°
• γ: 71.534 ± 0.002°
• Cell volume: 2574.7 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0766
• Residual factor for significantly intense reflections: 0.0456
• Weighted residual factors for significantly intense reflections: 0.1057
• Weighted residual factors for all reflections included in the refinement: 0.125
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No