Synthesis, structures and ring-opening polymerization studies of new zinc chloride and amide complexes supported by amidinate heteroscorpionate ligands
Authors of publication
Sánchez-Barba, Luis F.; Alonso-Moreno, Carlos; Garcés, Andrés; Fajardo, Mariano; Fernández-Baeza, Juan; Otero, Antonio; Lara-Sánchez, Agustín; Rodríguez, Ana M.; López-Solera, Isabel
Journal of publication
Dalton Transactions
Year of publication
2009
Journal issue
38
Pages of publication
8054 - 8062
a
8.3079 ± 0.0012 Å
b
19.091 ± 0.003 Å
c
16.587 ± 0.002 Å
α
90°
β
97.208 ± 0.003°
γ
90°
Cell volume
2610 ± 0.6 Å3
Cell temperature
180 ± 2 K
Ambient diffraction temperature
180 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.1053
Residual factor for significantly intense reflections
0.055
Weighted residual factors for significantly intense reflections
0.1282
Weighted residual factors for all reflections included in the refinement
0.1509
Goodness-of-fit parameter for all reflections included in the refinement
