Information card for entry 7002360

Structure parameters

• Formula: C30 H34 Cl2 N10 O13 Pd2
• Calculated formula: C30 H34 Cl2 N10 O13 Pd2
• Title of publication: 1H NMR spectroscopic identification of binding modes of 2,2′-bipyridine ligands in complexes of square-planar d8 metal ions
• Authors of publication: Shen, Wei-Zheng; Trötscher-Kaus, Gabriele; Lippert, Bernhard
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 39
• Pages of publication: 8203 - 8214
• a: 13.762 ± 0.003 Å
• b: 24.089 ± 0.005 Å
• c: 11.85 ± 0.002 Å
• α: 90°
• β: 112.13 ± 0.03°
• γ: 90°
• Cell volume: 3639 ± 1.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0903
• Residual factor for significantly intense reflections: 0.0513
• Weighted residual factors for significantly intense reflections: 0.126
• Weighted residual factors for all reflections included in the refinement: 0.1332
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No