Information card for entry 7002395

Structure parameters

• Formula: C18 H22 N8 Pb S2
• Calculated formula: C18 H22 N8 Pb S2
• SMILES: c1(cccc[n]12)C=[N]3N=C(S[Pb]2314SC(=N[N]1=Cc1cccc[n]14)NCC)NCC
• Title of publication: Coordinative trends of a tridentate thiosemicarbazone ligand: synthesis, characterization, luminescence studies and desulfurization processes
• Authors of publication: Pedrido, Rosa; Romero, María J.; Bermejo, Manuel R.; Martínez-Calvo, Miguel; González-Noya, Ana M.; Zaragoza, Guillermo
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 39
• Pages of publication: 8329 - 8340
• a: 14.194 ± 0.002 Å
• b: 13.2451 ± 0.0017 Å
• c: 12.1918 ± 0.0019 Å
• α: 90°
• β: 109.195 ± 0.007°
• γ: 90°
• Cell volume: 2164.6 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0625
• Weighted residual factors for significantly intense reflections: 0.1557
• Weighted residual factors for all reflections included in the refinement: 0.1651
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No