Information card for entry 7002457

Structure parameters

• Formula: C56 H47 Br2 Cl2 N2 O1.5 P2 Pd2
• Calculated formula: C55.75 H42 Br2 Cl2 N2 O1.5 P2 Pd2
• Title of publication: Synthesis and structures of complexes with axially chiral isoquinolinyl-naphtholate ligands
• Authors of publication: Howard, Ruth H.; Alonso-Moreno, Carlos; Broomfield, Lewis M.; Hughes, David L.; Wright, Joseph A.; Bochmann, Manfred
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 40
• Pages of publication: 8667 - 8682
• a: 11.3491 ± 0.0008 Å
• b: 13.3734 ± 0.001 Å
• c: 18.5704 ± 0.0008 Å
• α: 109.028 ± 0.006°
• β: 99.561 ± 0.005°
• γ: 99.732 ± 0.006°
• Cell volume: 2551.1 ± 0.3 ų
• Cell temperature: 140 ± 1 K
• Ambient diffraction temperature: 140 ± 1 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0518
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.1009
• Weighted residual factors for all reflections included in the refinement: 0.1052
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No