Information card for entry 7002744

Structure parameters

• Common name: Oxo-propoxo-(salicylaldehyde 4-phenylthiosemicarbazonato(2- ))vanadium(V)
• Formula: C17 H18 N3 O3 S V
• Calculated formula: C17 H18 N3 O3 S V
• Title of publication: Vanadium-induced formation of thiadiazole and thiazoline compounds. Mononuclear and dinuclear oxovanadium(v) complexes with open-chain and cyclized thiosemicarbazone ligands
• Authors of publication: Rubčić, Mirta; Milić, Dalibor; Horvat, Gordan; Đilović, Ivica; Galić, Nives; Tomišić, Vladislav; Cindrić, Marina
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 44
• Pages of publication: 9914 - 9923
• a: 15.1837 ± 0.0004 Å
• b: 8.0325 ± 0.0002 Å
• c: 16.0582 ± 0.0005 Å
• α: 90°
• β: 114.404 ± 0.004°
• γ: 90°
• Cell volume: 1783.52 ± 0.1 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0401
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.077
• Weighted residual factors for all reflections included in the refinement: 0.0806
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No