Information card for entry 7002749

Structure parameters

• Chemical name: poly-(pentakis(mu-cyanido)-(diethylenetriamine-k3N,N',N'') dicopper(I/II)-nickel(II)
• Formula: C9 H13 Cu2 N8 Ni
• Calculated formula: C9 H13 Cu2 N8 Ni
• Title of publication: Condensed heterometallic bidimensional mixed valence CuI/CuII/NiII cyanidometallate
• Authors of publication: Beobide, Garikoitz; Castillo, Oscar; Cepeda, Javier; Luque, Antonio; Pérez-Yáñez, Sonia; Román, Pascual
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 44
• Pages of publication: 9722 - 9724
• a: 12.8823 ± 0.0003 Å
• b: 8.682 ± 0.0002 Å
• c: 13.3457 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1492.64 ± 0.06 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0379
• Residual factor for significantly intense reflections: 0.0267
• Weighted residual factors for significantly intense reflections: 0.0621
• Weighted residual factors for all reflections included in the refinement: 0.0636
• Goodness-of-fit parameter for all reflections included in the refinement: 0.943
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No