Information card for entry 7002854

Structure parameters

• Formula: C32 H20 Fe5 N4 O16 Re2
• Calculated formula: C32 H20 Fe5 N4 O16 Re2
• Title of publication: Heterometallic complexes involving iron(ii) and rhenium(vii) centers connected by μ-oxido bridges
• Authors of publication: Gonçalves, Isabel S.; Lopes, André D.; Amarante, Tatiana R.; Paz, Filipe A. Almeida; Silva, Nuno J. O.; Pillinger, Martyn; Gago, Sandra; Palacio, Fernando; Kühn, Fritz E.; Romão, Carlos C.
• Journal of publication: Dalton Transactions
• Year of publication: 2009
• Journal issue: 46
• Pages of publication: 10199 - 10207
• a: 12.235 ± 0.004 Å
• b: 11.833 ± 0.004 Å
• c: 14.492 ± 0.005 Å
• α: 90°
• β: 105.606 ± 0.016°
• γ: 90°
• Cell volume: 2020.8 ± 1.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0476
• Residual factor for significantly intense reflections: 0.0328
• Weighted residual factors for significantly intense reflections: 0.0693
• Weighted residual factors for all reflections included in the refinement: 0.0748
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No