Information card for entry 7003129

Structure parameters

• Formula: C30 H140 N30 Ni8 O72 P2 W18
• Calculated formula: C30 H76 N30 Ni8 O72 P2 W18
• Title of publication: Two extended structures constructed from sandwich-type polyoxometalates functionalized by organic amines
• Authors of publication: Zhang, Zhiming; Liu, Jia; Wang, Enbo; Qin, Chao; Li, Yangguang; Qi, Yanfei; Wang, Xinlong
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 4
• Pages of publication: 463 - 468
• a: 13.302 ± 0.003 Å
• b: 13.882 ± 0.003 Å
• c: 17.039 ± 0.003 Å
• α: 67.79 ± 0.03°
• β: 71.34 ± 0.03°
• γ: 88.21 ± 0.03°
• Cell volume: 2745.4 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0629
• Residual factor for significantly intense reflections: 0.0489
• Weighted residual factors for significantly intense reflections: 0.1124
• Weighted residual factors for all reflections included in the refinement: 0.1195
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No