Information card for entry 7003139

Structure parameters

• Formula: C32 H32 B Cl1.11 N2
• Calculated formula: C32 H32 B Cl1.108 N2
• Title of publication: Light group 13 chloride diazadiene complexes: consequences of varying substituent bulk
• Authors of publication: Hinchliffe, Alan; Mair, Francis S.; McInnes, Eric J. L.; Pritchard, Robin G.; Warren, John E.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 2
• Pages of publication: 222 - 233
• a: 21.7735 ± 0.0014 Å
• b: 9.7868 ± 0.0007 Å
• c: 13.2216 ± 0.001 Å
• α: 90°
• β: 99.065 ± 0.004°
• γ: 90°
• Cell volume: 2782.2 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0964
• Residual factor for significantly intense reflections: 0.0552
• Weighted residual factors for significantly intense reflections: 0.1078
• Weighted residual factors for all reflections included in the refinement: 0.123
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No