Information card for entry 7003204

Structure parameters

• Formula: H34 N2 Na4 O74 V3 W17
• Calculated formula: N2 Na4 O74 V2 W17.28
• Title of publication: Bridging the gap between solution and solid state studies in polyoxometalate chemistry: Discovery of a family of [V1M17]-based cages encapsulating two {VVO4} moieties
• Authors of publication: Miras, Haralampos N.; Long, De-Liang; Kögerler, Paul; Cronin, Leroy
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 2
• Pages of publication: 214 - 221
• a: 23.414 ± 0.002 Å
• b: 37.666 ± 0.004 Å
• c: 13.0008 ± 0.0013 Å
• α: 90°
• β: 111.81 ± 0.003°
• γ: 90°
• Cell volume: 10644.9 ± 1.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.093
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for significantly intense reflections: 0.1292
• Weighted residual factors for all reflections included in the refinement: 0.1517
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No