Information card for entry 7003771

Structure parameters

• Formula: C18 H48 B10 O0.12 P2
• Calculated formula: C18 H47.882 B10 O0.118 P2
• Title of publication: A simple entry into nido-C2B10 clusters: HCl promoted cleavage of the C‒C bond in ortho-carboranyl diphosphines
• Authors of publication: Charmant, Jonathan P. H.; Haddow, Mairi F.; Mistry, Rakesh; Norman, Nicholas C.; Orpen, A. Guy; Pringle, Paul G.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 11
• Pages of publication: 1409 - 1411
• a: 8.964 ± 0.003 Å
• b: 10.496 ± 0.003 Å
• c: 15.234 ± 0.004 Å
• α: 70.82 ± 0.02°
• β: 80.68 ± 0.02°
• γ: 89.78 ± 0.03°
• Cell volume: 1334 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0805
• Residual factor for significantly intense reflections: 0.0678
• Weighted residual factors for significantly intense reflections: 0.1747
• Weighted residual factors for all reflections included in the refinement: 0.1892
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No