Information card for entry 7004033

Structure parameters

• Formula: C10 H18 Cl5 Cu0.5 N4 O2 Re
• Calculated formula: C10 H18 Cl5 Cu0.5 N4 O2 Re
• Title of publication: Pentachloro(pyrazine)rhenate(iv) complex as precursor of heterobimetallic pyrazine-containing ReIV2MII (M = Ni, Cu) species: synthesis, crystal structures and magnetic properties
• Authors of publication: Martínez-Lillo, José; Armentano, Donatella; Marino, Nadia; Arizaga, Livia; Chiozzone, Raúl; González, Ricardo; Kremer, Carlos; Cano, Joan; Faus, Juan
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 34
• Pages of publication: 4585
• a: 9.4579 ± 0.0003 Å
• b: 10.2914 ± 0.0003 Å
• c: 11.8237 ± 0.0004 Å
• α: 109.361 ± 0.001°
• β: 99.969 ± 0.001°
• γ: 102.096 ± 0.001°
• Cell volume: 1024.31 ± 0.06 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0207
• Residual factor for significantly intense reflections: 0.0187
• Weighted residual factors for significantly intense reflections: 0.0449
• Weighted residual factors for all reflections included in the refinement: 0.0458
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No