Information card for entry 7004096

Structure parameters

• Formula: C52 H62 F8 N24 Ni2 O51 Si W12
• Calculated formula: C52 H48 F8 N24 Ni2 O51 Si W11.98
• Title of publication: Construction of different dimensional inorganic‒organic hybrid materials based on polyoxometalates and metal‒organic units via changing metal ions: from non-covalent interactions to covalent connections
• Authors of publication: Lan, Ya-Qian; Li, Shun-Li; Shao, Kui-Zhan; Wang, Xin-Long; Su, Zhong-Min
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 29
• Pages of publication: 3824 - 3835
• a: 14.6355 ± 0.0004 Å
• b: 21.0669 ± 0.0005 Å
• c: 16.3476 ± 0.0008 Å
• α: 90°
• β: 98.291 ± 0.001°
• γ: 90°
• Cell volume: 4987.7 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0805
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1186
• Weighted residual factors for all reflections included in the refinement: 0.1338
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No