Information card for entry 7004277

Structure parameters

• Common name: [Ru4(mu4-S)2(CO)9(IMes)2]2THF
• Formula: C29.5 H32 N2 O5.5 Ru2 S
• Calculated formula: C29.5 H32 N2 O5.5 Ru2 S
• Title of publication: The reactivity of N-heterocyclic carbenes and their precursors with [Ru3(CO)12]
• Authors of publication: Bruce, Michael I.; Cole, Marcus L.; Fung, Ricky S. C.; Forsyth, Craig M.; Hilder, Matthias; Junk, Peter C.; Konstas, Kristina
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 31
• Pages of publication: 4118 - 4128
• a: 10.7389 ± 0.0001 Å
• b: 22.2879 ± 0.0003 Å
• c: 24.3237 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5821.82 ± 0.12 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.0738
• Residual factor for significantly intense reflections: 0.0452
• Weighted residual factors for significantly intense reflections: 0.1112
• Weighted residual factors for all reflections included in the refinement: 0.1271
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No