Information card for entry 7004710

Structure parameters

• Formula: C49 H48.5 F18 Fe N15.5 O2.5 P3
• Calculated formula: C49 H43.5 F18 Fe N15.5 O2.5 P3
• Title of publication: Curly‒curly, loop‒loop: homoleptic metal(ii) complexes of pyridinecarbaldehyde 4′-(2,2′:6′,2″-terpyridyl)hydrazones and their coordination polymers
• Authors of publication: Beves, Jonathon E.; Constable, Edwin C.; Housecroft, Catherine E.; Kepert, Cameron J.; Neuburger, Markus; Price, David J.; Schaffner, Silvia; Zampese, Jennifer A.
• Journal of publication: Dalton Transactions
• Year of publication: 2008
• Journal issue: 47
• Pages of publication: 6742 - 6751
• a: 8.8794 ± 0.0018 Å
• b: 16.055 ± 0.003 Å
• c: 23.71 ± 0.005 Å
• α: 105.43 ± 0.03°
• β: 91.68 ± 0.03°
• γ: 97.54 ± 0.03°
• Cell volume: 3222.8 ± 1.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1226
• Residual factor for significantly intense reflections: 0.0952
• Weighted residual factors for significantly intense reflections: 0.2477
• Weighted residual factors for all reflections included in the refinement: 0.2723
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7004703
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No