Information card for entry 7004904

Structure parameters

• Formula: C74 H122 N4 O4 Yb2
• Calculated formula: C74 H122 N4 O4 Yb2
• Title of publication: Synthesis, structure and oxidation of new ytterbium(II) bis(phenolate) compounds and their catalytic activity towards epsilon-caprolactone.
• Authors of publication: Delbridge, Ewan E.; Dugah, Divine T.; Nelson, Chassidy R.; Skelton, Brian W.; White, Allan H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 1
• Pages of publication: 143 - 153
• a: 14.049 ± 0.005 Å
• b: 9.693 ± 0.005 Å
• c: 26.772 ± 0.008 Å
• α: 90°
• β: 91.352 ± 0.005°
• γ: 90°
• Cell volume: 3645 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.088
• Residual factor for significantly intense reflections: 0.063
• Weighted residual factors for all reflections: 0.167
• Weighted residual factors for all reflections included in the refinement: 0.129
• Goodness-of-fit parameter for all reflections: 1.217
• Goodness-of-fit parameter for all reflections included in the refinement: 1.217
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No