Information card for entry 7004981

Structure parameters

• Common name: [Al{Me3SiNC(PhMe)NPh}2(Cl/Me)]
• Formula: C34.52 H43.56 Al Cl0.48 N4 Si2
• Calculated formula: C34.521 H42 Al Cl0.479 N4 Si2
• Title of publication: Synthesis and structures of selected benzamidinates of Li, Na, Al, Zr and Sn(II) using the C1-symmetric ligands [N(SiMe3)C(C6H4Me-4 or Ph)NPh]-.
• Authors of publication: Hitchcock, Peter B.; Lappert, Michael F.; Merle, Philippe G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 5
• Pages of publication: 585 - 594
• a: 10.2505 ± 0.0003 Å
• b: 12.4069 ± 0.0003 Å
• c: 14.8217 ± 0.0003 Å
• α: 105.102 ± 0.001°
• β: 101.05 ± 0.001°
• γ: 93.509 ± 0.001°
• Cell volume: 1773.81 ± 0.08 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0556
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1088
• Weighted residual factors for all reflections included in the refinement: 0.117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No