Information card for entry 7005243

Structure parameters

• Formula: C81 H82 Cl2 O8 P4 Ru2
• Calculated formula: C80.866 H78.72 Cl2 O8 P4 Ru2
• Title of publication: Bis(acetylacetonato)ruthenium(II) complexes containing alkynyldiphenylphosphines. Formation and redox behaviour of [Ru(acac)2(Ph2PC triple bond CR)2] (R=H, Me, Ph) complexes and the binuclear complex cis-[{Ru(acac)2}2(micro-Ph2PC triple bond CPPh2)}2].
• Authors of publication: Bennett, Martin A.; Byrnes, Matthew J.; Willis, Anthony C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 17
• Pages of publication: 1677 - 1686
• a: 16.317 ± 0.004 Å
• b: 16.469 ± 0.006 Å
• c: 18.975 ± 0.004 Å
• α: 65.46 ± 0.02°
• β: 66.17 ± 0.02°
• γ: 60.76 ± 0.02°
• Cell volume: 3915 ± 2 ų
• Cell temperature: 296.2 K
• Ambient diffraction temperature: 296.2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1292
• Residual factor for significantly intense reflections: 0.0417
• Weighted residual factors for all reflections: 0.0547
• Weighted residual factors for significantly intense reflections: 0.0439
• Weighted residual factors for all reflections included in the refinement: 0.0439
• Goodness-of-fit parameter for all reflections: 1.323
• Goodness-of-fit parameter for all reflections included in the refinement: 1.538
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No