Information card for entry 7005273

Structure parameters

• Formula: C16 H26 Br1.71 Cl0.29 Ge Sn W
• Calculated formula: C16 H26 Br1.71 Cl0.29 Ge Sn W
• Title of publication: Synthesis and structural studies of germyl and germyl/stannyl substituted tungstenocenes
• Authors of publication: Khalimon, Andrey Yu.; Dorogov, Konstantin Yu.; Churakov, Andrei V.; Kuzmina, Lyudmila G.; Lemenovskii, Dmitry A.; Howard, Judith A. K.; Nikonov, Georgii I.
• Journal of publication: Dalton Transactions
• Year of publication: 2007
• Journal issue: 23
• Pages of publication: 2440
• a: 15.5322 ± 0.0003 Å
• b: 8.7717 ± 0.0002 Å
• c: 14.2873 ± 0.0002 Å
• α: 90°
• β: 90.741 ± 0.001°
• γ: 90°
• Cell volume: 1946.39 ± 0.06 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0401
• Residual factor for significantly intense reflections: 0.0375
• Weighted residual factors for significantly intense reflections: 0.1155
• Weighted residual factors for all reflections included in the refinement: 0.1171
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No