Information card for entry 7005332

Structure parameters

• Formula: C54 H82 F3 I3 N7.5 O3 P0.5 Rh2
• Calculated formula: C54 H82 F3 I3 N7.5 O3 P0.5 Rh2
• Title of publication: Iodination of triazenide-bridged rhodium and iridium complexes: oxidative addition vs. one-electron oxidation.
• Authors of publication: Adams, Christopher J.; Baber, R. Angharad; Connelly, Neil G.; Harding, Phimphaka; Hayward, Owen D.; Kandiah, Mathivathani; Orpen, A. Guy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 13
• Pages of publication: 1325 - 1333
• a: 30.696 ± 0.004 Å
• b: 11.6049 ± 0.0015 Å
• c: 18.233 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6495 ± 1.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for all reflections: 0.0839
• Residual factor for significantly intense reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.1148
• Weighted residual factors for all reflections included in the refinement: 0.1389
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No