Neutral (bis-beta-diketonato) iron(III), cobalt(II), nickel(II), copper(II) and zinc(II) metallocycles: structural, electrochemical and solvent extraction studies.
Authors of publication
Clegg, Jack K.; Bray, David J.; Gloe, Kerstin; Gloe, Karsten; Hayter, Michael J.; Jolliffe, Katrina A.; Lawrance, Geoffrey A.; Meehan, George V.; McMurtrie, John C.; Lindoy, Leonard F.; Wenzel, Marco
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2007
Journal issue
17
Pages of publication
1719 - 1730
a
12.204 ± 0.0016 Å
b
17.332 ± 0.002 Å
c
18.061 ± 0.002 Å
α
117.185 ± 0.002°
β
99.516 ± 0.002°
γ
102.001 ± 0.002°
Cell volume
3171.7 ± 0.7 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.086
Residual factor for significantly intense reflections
0.051
Weighted residual factors for significantly intense reflections
0.1368
Weighted residual factors for all reflections included in the refinement
0.1594
Goodness-of-fit parameter for all reflections included in the refinement
