Information card for entry 7005467

Structure parameters

• Formula: C50 H62 Ag4 Cl6 N16 O4 S4
• Calculated formula: C50 H60 Ag4 Cl6 N16 O4 S4
• Title of publication: Synthesis, reaction and structure of a highly light-stable silver(I) cluster with an Ag4S4N4 core having a tridentate 4N-morpholyl 2-acetylpyridine thiosemicarbazone ligand: use of water-soluble silver(I) carboxylates as a silver(I) source.
• Authors of publication: Onodera, Kuniaki; Kasuga, Noriko Chikaraishi; Takashima, Tomomi; Hara, Akihiro; Amano, Akifumi; Murakami, Hideyuki; Nomiya, Kenji
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 33
• Pages of publication: 3646 - 3652
• a: 9.997 ± 0.004 Å
• b: 11.983 ± 0.005 Å
• c: 13.481 ± 0.006 Å
• α: 73.203 ± 0.006°
• β: 87.14 ± 0.006°
• γ: 85.074 ± 0.006°
• Cell volume: 1539.8 ± 1.1 ų
• Cell temperature: 90 K
• Ambient diffraction temperature: 90 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0345
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for significantly intense reflections: 0.0814
• Weighted residual factors for all reflections included in the refinement: 0.0928
• Goodness-of-fit parameter for all reflections included in the refinement: 1.132
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No