Information card for entry 7005835

Structure parameters

• Formula: Bi2 H102 Na14 O119 W18 Zn4
• Calculated formula: Bi2 Na14 O114 W18 Zn4
• Title of publication: The novel sandwich-type heteropolyoxotungstates [M2Bi2(beta-B-MW9O34)2]14- (M = Co(II), Zn(II)): beta-type dimeric heteropolyanions with a transition metal as the central heteroatom and Bi(III) and M as linking atoms.
• Authors of publication: Liu, Ying; Liu, Bin; Xue, Ganglin; Hu, Huaiming; Fu, Feng; Wang, Jiwu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 33
• Pages of publication: 3634 - 3639
• a: 13.6266 ± 0.0016 Å
• b: 14.3963 ± 0.0017 Å
• c: 15.3377 ± 0.0018 Å
• α: 65.66 ± 0.001°
• β: 89.667 ± 0.002°
• γ: 71.745 ± 0.002°
• Cell volume: 2576.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0936
• Residual factor for significantly intense reflections: 0.0723
• Weighted residual factors for significantly intense reflections: 0.1897
• Weighted residual factors for all reflections included in the refinement: 0.2066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No