Information card for entry 7005910

Structure parameters

• Formula: C40 H248 K15 Li15 O282 P8 Ru4 W49
• Calculated formula: C40 H56 K9 O240 P8 Ru4 W49
• Title of publication: Organoruthenium derivative of the cyclic [H7P8W48O184]33- anion: [{K(H2O)}3{Ru(p-cymene)(H2O)}4P8W49O186(H2O)2]27-.
• Authors of publication: Mal, Sib Sankar; Nsouli, Nadeen H.; Dickman, Michael H.; Kortz, Ulrich
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2007
• Journal issue: 25
• Pages of publication: 2627 - 2630
• a: 19.0968 ± 0.0012 Å
• b: 20.2604 ± 0.0012 Å
• c: 22.6082 ± 0.001 Å
• α: 101.977 ± 0.003°
• β: 109.431 ± 0.003°
• γ: 100.737 ± 0.003°
• Cell volume: 7754.3 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1141
• Residual factor for significantly intense reflections: 0.065
• Weighted residual factors for significantly intense reflections: 0.1742
• Weighted residual factors for all reflections included in the refinement: 0.2121
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No