Crystallography Open Database

Information card for entry 7006016

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Structure parameters

Formula	C30 H86 B2 K2 N4 P2 Si4
Calculated formula	C30 H86 B2 K2 N4 P2 Si4
Title of publication	Alkali metal complexes of a phosphine-borane-stabilised carbanion: influence of co-ligands on structure.
Authors of publication	Izod, Keith; Wills, Corinne; Clegg, William; Harrington, Ross W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2007
Journal issue	33
Pages of publication	3669 - 3675
a	8.7353 ± 0.0006 Å
b	11.3832 ± 0.0008 Å
c	13.5668 ± 0.001 Å
α	79.174 ± 0.001°
β	79.418 ± 0.001°
γ	71.435 ± 0.001°
Cell volume	1244.9 ± 0.15 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0551
Residual factor for significantly intense reflections	0.0518
Weighted residual factors for significantly intense reflections	0.1167
Weighted residual factors for all reflections included in the refinement	0.1185
Goodness-of-fit parameter for all reflections included in the refinement	1.152
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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